HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 86750329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 86750327 | HCID 86750327 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86750329 | HCID 86750329 | 55.8% |
Reaction Steps
A mixture of 0.80 g of product from Example 57, 0.431 g of sodium iodide and 20 ml of acetone is heated at reflux temperature for 5 days. The reaction is concentrated in vacuo and the residue purified by chromatography (silica Gel: 80% ethyl acetate/hexane) to give 0.472 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750735 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-53ae8808da5e47f58108bf281ff56d3a |
| Source note | uspto-grants-1998_05 |