HCID 21218301, compound → HCID 21218289, compound

HRID 1290569Notes

Reaction equation

HRID 1290569 reaction equation
[N+:1]([C:4]1[CH:12]=[CH:11][C:10]([CH2:13][CH3:14])=[C:9]2[C:5]=1[CH2:6][CH2:7][NH:8]2)([O-])=O.[N+](C1C(CC)=C2C(CCN2)=CC=1)([O-])=O>>[NH2:1][C:4]1[CH:12]=[CH:11][C:10]([CH2:13][CH3:14])=[C:9]2[C:5]=1[CH:6]=[CH:7][NH:8]2

Participants

3

Reactant 2

HCID 21218301HCID 21218301, compoundHCID 21218307HCID 21218307, compound

Product 1

HCID 21218289HCID 21218289, compound

Procedure

4-nitro 7-ethylindoline was reduced in the same manner than 6-nitro 7-ethylindoline. 6 g of indole recrystallized from a ethylacetate/isopropylic ether (1/3) mixture were obtained.

Workup

  1. custom6 g of indole recrystallized from a ethylacetate/isopropylic ether (1/3) mixture
  2. customwere obtained

Sources & evidence

ORD record
ord-8797b4d4b2fb422fb166be5ad566b3c4
Source dataset
uspto-grants-1998_05
Patent number
US05752982

Reaction notes

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