3,5-Dichlorobenzoyl chloride → HCID 18916081, compound

HRID 1290587Notes

Reaction equation

HRID 1290587 reaction equation
[N+](C1C=CC(C([N:10]2[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][C:11]2=[O:17])=O)=CC=1)([O-])=O.[Cl:20][C:21]1[CH:22]=[C:23]([CH:27]=[C:28]([Cl:30])[CH:29]=1)[C:24](Cl)=[O:25]>>[Cl:20][C:21]1[CH:22]=[C:23]([CH:27]=[C:28]([Cl:30])[CH:29]=1)[C:24]([N:10]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][C:11]1=[O:17])=[O:25]

Participants

3

Reactant 2

HCID 761913,5-Dichlorobenzoyl chlorideHCID 8274182H-Azepin-2-one, hexahydro-1-(4-nitrobenzoyl)-

Product 1

HCID 18916081HCID 18916081, compound

Procedure

Synthesized as for N-(4-nitrobenzoyl)caprolactam (Example XXIII) using 3,5-dichlorobenzoylchloride (Aldrich) in place of 4-nitrobenzoyl chloride.

Sources & evidence

ORD record
ord-8a73483b485d4378b5686d2f4acb400e
Source dataset
uspto-grants-1998_05
Patent number
US05753138

Reaction notes

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