Benzoyl chloride, 3-nitro- → HCID 18916095, compound

HRID 1290590Notes

Reaction equation

HRID 1290590 reaction equation
[N+]([C:4]1[CH:19]=[CH:18][C:7]([C:8]([N:10]2[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][C:11]2=[O:17])=[O:9])=[CH:6][CH:5]=1)([O-])=O.[N+:20](C1C=C(C=CC=1)C(Cl)=O)([O-:22])=[O:21]>>[N+:20]([C:19]1[CH:18]=[C:7]([CH:6]=[CH:5][CH:4]=1)[C:8]([N:10]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][C:11]1=[O:17])=[O:9])([O-:22])=[O:21]

Participants

3

Reactant 2

HCID 8495Benzoyl chloride, 3-nitro-HCID 8274182H-Azepin-2-one, hexahydro-1-(4-nitrobenzoyl)-

Product 1

HCID 18916095HCID 18916095, compound

Procedure

Synthesized as for N-(4-nitrobenzoyl)caprolactam (Example XXIII) using 3-nitrobenzoyl chloride (Aldrich) in place of 4-nitrobenzoyl chloride.

Sources & evidence

ORD record
ord-b23553f96abd4c42bc5377227c9493af
Source dataset
uspto-grants-1998_05
Patent number
US05753138

Reaction notes

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