4-Chlorobenzoyl chloride → ST50050739

HRID 1290593Notes

Reaction equation

HRID 1290593 reaction equation
[N+]([C:4]1[CH:19]=[CH:18][C:7]([C:8]([N:10]2[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][C:11]2=[O:17])=[O:9])=[CH:6][CH:5]=1)([O-])=O.[Cl:20]C1C=CC(C(Cl)=O)=CC=1>>[Cl:20][C:4]1[CH:19]=[CH:18][C:7]([C:8]([N:10]2[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][C:11]2=[O:17])=[O:9])=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 85014-Chlorobenzoyl chlorideHCID 8274182H-Azepin-2-one, hexahydro-1-(4-nitrobenzoyl)-

Product 1

HCID 703952ST50050739

Procedure

Synthesized as for N-(4-nitrobenzoyl)caprolactam (Example XXIII) using 4-chlorobenzoylchloride (Aldrich) in place of 4-nitrobenzoyl chloride.

Sources & evidence

ORD record
ord-1ec019c29d5c49a08317611379b94f59
Source dataset
uspto-grants-1998_05
Patent number
US05753138

Reaction notes

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