HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1-(6-hydrazinyl-3-pyridinyl)pyrrole-2,5-dione;hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 2-Chloro-5-nitropyridine | HCID 78308 | — |
| Reactant | Di-tert-butyl dicarbonate | HCID 90495 | — |
| Catalyst | Cobalt diacetate | HCID 6277 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 1-(6-hydrazinyl-3-pyridinyl)pyrrole-2,5-dione;hydrochloride | HCID 178479591 | — |
Reaction Steps
2-chloro-5-nitropyridine, hydrazine hydrate, di-tert-butyl dicarbonate, 10% palladium on charcoal, maleic anhydride, cobalt acetate and acetic anhydride were purchased from Aldrich Chemicals (Milwaukee, Wis.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753520 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-970ef3a3db434275abf8ee2f98bb2026 |
| Source note | uspto-grants-1998_05 |