Aluminium lithium hydride → HCID 15289115, compound
Reaction equation
[CH2:1]([N:3]([CH2:17]C)[C:4]12[CH2:14][CH2:13][CH:10]([CH:11]=[CH:12]1)[CH:9]1[CH:5]2[C:6](=O)[NH:7][C:8]1=O)C.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[CH3:1][N:3]([CH3:17])[C:4]12[CH2:14][CH2:13][CH:10]([CH:11]=[CH:12]1)[CH:9]1[CH:5]2[CH2:6][NH:7][CH2:8]1Participants
3
Procedure
12 g (54.5 mmol) of 1-diethylamino-4-azatricyclo-[5.2.2.02,6 ]undec-8-ene-3,5-dione are reduced with LiAlH4 as described under Z 1-B and the mixture is worked up accordingly.
Sources & evidence
- ORD record
- ord-9b5c5bc0f2634fae813e275b7d74740e
- Source dataset
- uspto-grants-1998_05
- Patent number
- US05753669
Reaction notes
Loading…