Aluminium lithium hydride → HCID 15289115, compound

HRID 1290853Notes

Reaction equation

HRID 1290853 reaction equation
[CH2:1]([N:3]([CH2:17]C)[C:4]12[CH2:14][CH2:13][CH:10]([CH:11]=[CH:12]1)[CH:9]1[CH:5]2[C:6](=O)[NH:7][C:8]1=O)C.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[CH3:1][N:3]([CH3:17])[C:4]12[CH2:14][CH2:13][CH:10]([CH:11]=[CH:12]1)[CH:9]1[CH:5]2[CH2:6][NH:7][CH2:8]1

Participants

3

Procedure

12 g (54.5 mmol) of 1-diethylamino-4-azatricyclo-[5.2.2.02,6 ]undec-8-ene-3,5-dione are reduced with LiAlH4 as described under Z 1-B and the mixture is worked up accordingly.

Sources & evidence

ORD record
ord-9b5c5bc0f2634fae813e275b7d74740e
Source dataset
uspto-grants-1998_05
Patent number
US05753669

Reaction notes

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