HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylmaleimide → HCID 15289129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylmaleimide | HCID 74204 | — |
| Reactant | HCID 15289128 | HCID 15289128 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 15289129 | HCID 15289129 | — |
Reaction Steps
32.8 g (0.17 mol) of N-benzylmaleimide are heated under reflux with 24.2 g (0.17 mol) of diethyl tricyclo[5.2.1.02,6 ]deca-3,8-diene-1,4-dicarboxylate in 200 ml of 1,4-dioxane overnight. The mixture is concentrated, the residue is taken up in 80 ml of isopropanol and the product is allowed to crystallize out.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753669 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-90ad51910e50413ab41156ff429d12ac |
| Source note | uspto-grants-1998_05 |