HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 22857244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | HCID 54000904 | HCID 54000904 | — |
| Product | HCID 22857244 | HCID 22857244 | — |
Reaction Steps
Benzyl 2,4-di-O-acetyl-3,6-dideoxychloroacetamido-alpha-D-mannopyranoside, 20, 0.65 g (0.00157 mole) and triethyl phosphite (5 mL) were heated at 110°-120° C. for 4.5 h with stirring under argon. The solvent was distilled at high vacuum, 50 mg of the residue was saved, and the rest carried on.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05466809 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-448fce20f3d84643a5c72ba2736690cf |
| Source note | uspto-grants-1995_11 |