Methyl iodide → HCID 19075349, compound

HRID 1291450Notes

Reaction equation

HRID 1291450 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:12]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH2:4][CH:5]=[CH2:6]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:12]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH2:4][CH:5]=[CH2:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075515HCID 19075515, compound

Product 1

HCID 19075349HCID 19075349, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and 3-(3-(3-butenyloxy)-1,2,5-thiadiazol-4-yl)pyridine (583 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 890 mg (96%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 890 mg (96%)

Sources & evidence

ORD record
ord-e125b6e5803e4819be655832363321dd
Source dataset
uspto-grants-1998_05
Patent number
US05753683

Reaction notes

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