Methyl iodide → HCID 70146039, compound

HRID 1291475Notes

Reaction equation

HRID 1291475 reaction equation
[CH3:1][I:2].[CH2:3]([O:9][C:10]1[C:14]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:13][S:12][N:11]=1)[CH2:4][CH2:5][CH:6]=[CH:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([O:9][C:10]1[C:14]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:13][S:12][N:11]=1)[CH2:4][CH2:5][CH:6]=[CH:7][CH3:8]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 54194020HCID 54194020, compound

Product 1

HCID 70146039HCID 70146039, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (1 ml, 15 mmol) and 3-(3-(4-hexenyloxy)-1,2, 5-thiadiazol-4-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.54 g (45%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.54 g (45%)

Sources & evidence

ORD record
ord-5132caf7de964f9f95624d04bdf377b5
Source dataset
uspto-grants-1998_05
Patent number
US05753683

Reaction notes

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