Methyl iodide → 3-(4-(2-(2-Ethoxyethoxy)ethoxy)-1,2,5-thiadiazol-3-yl)-1-methylpyridinium iodide

HRID 1291500Notes

Reaction equation

HRID 1291500 reaction equation
[CH3:1][I:2].[CH2:3]([O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][O:11][C:12]1[C:16]([C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[N:15][S:14][N:13]=1)[CH3:4]>CC(C)=O>[I-:2].[CH2:3]([O:5][CH2:6][CH2:7][O:8][CH2:9][CH2:10][O:11][C:12]1[C:16]([C:17]2[CH:18]=[N+:19]([CH3:1])[CH:20]=[CH:21][CH:22]=2)=[N:15][S:14][N:13]=1)[CH3:4]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 190754773-(3-(2-(2-Ethoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-yl)pyridine

Product 1

HCID 190753263-(4-(2-(2-Ethoxyethoxy)ethoxy)-1,2,5-thiadiazol-3-yl)-1-methylpyridinium iodide

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 9 mmol) and 3-(3-(2-(2-ethoxyethoxy)-ethoxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration.

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration

Sources & evidence

ORD record
ord-769c2797f2414f9ea32d1619b3ea195e
Source dataset
uspto-grants-1998_05
Patent number
US05753683

Reaction notes

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