Methyl iodide → HCID 19075292, compound
Reaction equation
[CH3:1][I:2].[CH3:3][S:4][C:5]1[C:9]([C:10]2[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=2)=[N:8][S:7][N:6]=1>>[I-:2].[CH3:3][S:4][C:5]1[C:9]([C:10]2[CH:11]=[N+:12]([CH3:1])[CH:13]=[CH:14][CH:15]=2)=[N:8][S:7][N:6]=1Participants
3
Procedure
Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-methylthio-1,2,5-thiadiazol-4-yl)pyridine (0.5 g, 2.3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.
Workup
- customevaporated
Sources & evidence
- ORD record
- ord-57ab000fc9914535963e12b769add77f
- Source dataset
- uspto-grants-1998_05
- Patent number
- US05753683
Reaction notes
Loading…