Methyl iodide → HCID 19075272, compound
Reaction equation
[CH3:1][I:2].[CH2:3]([S:8][C:9]1[C:13]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:12][S:11][N:10]=1)[CH2:4][CH2:5][CH2:6][CH3:7]>>[I-:2].[CH2:3]([S:8][C:9]1[C:13]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:12][S:11][N:10]=1)[CH2:4][CH2:5][CH2:6][CH3:7]Participants
3
Procedure
Methyl iodide (0.5 ml, 7.5 mmol) was added to a solution of 3-(3-pentylthio1,2,5-thiadiazol-4-yl)pyridine (3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.
Workup
- customevaporated
Sources & evidence
- ORD record
- ord-a8d727f033fa4a1e8f20b8a6943540d8
- Source dataset
- uspto-grants-1998_05
- Patent number
- US05753683
Reaction notes
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