Methyl iodide → HCID 19075299, compound

HRID 1291530Notes

Reaction equation

HRID 1291530 reaction equation
[CH3:1][I:2].[CH2:3]([S:9][C:10]1[C:14]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:13][S:12][N:11]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]>>[I-:2].[CH2:3]([S:9][C:10]1[C:14]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:13][S:12][N:11]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 10755149HCID 10755149, compound

Product 1

HCID 19075299HCID 19075299, compound

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-hexylthio-1,2, 5-thiadiazol-4-yl)pyridine (3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-a6a337d53186441382ce9f39339d3e73
Source dataset
uspto-grants-1998_05
Patent number
US05753683

Reaction notes

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