HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19607765, compound → HCID 10297101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19607765 | HCID 19607765 | — |
| Solvent | Diethyl ether methanol | HCID 21864698 | — |
| Product | HCID 10297101 | HCID 10297101 | 70.3% |
Reaction Steps
Using 5-dimethylamino-1-(2-methyl-4-aminobenzoyl)-2,3,4,5-tetrahydro-1H-benzazepine (G) (1.00 g), 5-dimethylamino-1-[2-methyl-4-(2-methylbenzoylamino)benzoyl]-2,3,4,5-tetrahydro-1H-benzazepine (0.48 g) is obtained in the same manner as in Example 978 except that methanol/diethyl ether is used instead of ethyl acetate as recrystallization solvent, as white powder, m.p. 183°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753677 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-cffa7f20d31c4eb690f06acec92336bf |
| Source note | uspto-grants-1998_05 |