HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Di-p-toluidinoterephthalic acid → 5,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Di-p-toluidinoterephthalic acid | HCID 82524 | — |
| Reactant | 2,5-Bis[4-(3,4-dimethyl-5-isoxazolyl)sulfamoylanilino]terephthalic acid | HCID 18913708 | — |
| Product | 5,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dione | HCID 70423 | — |
Reaction Steps
Pigmentary 2,9-dimethylquinacridone was prepared exactly as described in comparison Example 1 except that 10% by weight, relative to the 2,5-di(4-methylanilino)terephthalic acid, of 2,5-bis[4-(3,4-dimethyl-5-isoxazolyl)sulfamoylanilino]terephthalic acid (6.8 g) was included in the ring-closure reaction. 2,9-Dimethylquinacridone (59 g) was obtained as a magenta pigment.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05755873 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-2828cd0ae2f244e0b653849b0add670f |
| Source note | uspto-grants-1998_05 |