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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1291946Generated: October 25, 2026

2,5-Di-p-toluidinoterephthalic acid → 5,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dione

https://huagongshe.com/reaction/1291946

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,5-Di-p-toluidinoterephthalic acidHCID 82524—
Reactant2,5-Bis[4-(3,4-dimethyl-5-isoxazolyl)sulfamoylanilino]terephthalic acidHCID 18913708—
Product5,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dioneHCID 70423—

Reaction Steps

Pigmentary 2,9-dimethylquinacridone was prepared exactly as described in comparison Example 1 except that 10% by weight, relative to the 2,5-di(4-methylanilino)terephthalic acid, of 2,5-bis[4-(3,4-dimethyl-5-isoxazolyl)sulfamoylanilino]terephthalic acid (6.8 g) was included in the ring-closure reaction. 2,9-Dimethylquinacridone (59 g) was obtained as a magenta pigment.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05755873
Source datasetuspto-grants-1998_05
ORD IDord-2828cd0ae2f244e0b653849b0add670f
Source noteuspto-grants-1998_05