HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 129200Generated: October 29, 2026
Acetic Anhydride → 3-[2-(Acetyloxy)ethyl]dihydro-2(3H)-furanone
https://huagongshe.com/reaction/129200
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Dihydro-3-(2-methoxyethyl)-2(3H)-furanone | HCID 14228512 | — |
| Product | 3-[2-(Acetyloxy)ethyl]dihydro-2(3H)-furanone | HCID 11008384 | 61% |
Reaction Steps
In a stirred vessel, a mixture of 20 g of 3-(2'-methoxyethyl)-dihydro-2(3H)furanone, 100 g of acetic anhydride, and 10 of Nafion is heated to 120° C. Following a period of 69 h, the reaction is terminated (conversion: 100%) and the catalyst is separated by filtration. Following purification by distillation, there is obtained 61% of 3-(2'-acetoxyethyl)-dihydro-2(3H)furanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05466831 |
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| Source dataset | uspto-grants-1995_11 |
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| ORD ID | ord-9c71d9ee151e4b7183179eb079b0ae27 |
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| Source note | uspto-grants-1995_11 |
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