3,4-Diethoxybenzaldehyde → HCID 178466602, compound

HRID 1292016Notes

Reaction equation

HRID 1292016 reaction equation
[C@H:1]1([NH2:8])[CH2:6][CH2:5][C@H:4]([NH2:7])[CH2:3][CH2:2]1.[CH2:9]([O:11][C:12]1[CH:13]=[C:14]([CH:17]=[CH:18][C:19]=1[O:20][CH2:21][CH3:22])[CH:15]=O)[CH3:10]>>[CH2:9]([O:11][C:12]1[CH:13]=[C:14]([CH:17]=[CH:18][C:19]=1[O:20][CH2:21][CH3:22])[CH2:15][NH:7][C@H:4]1[CH2:5][CH2:6][C@H:1]([NH:8][CH2:15][C:14]2[CH:17]=[CH:18][C:19]([O:20][CH2:21][CH3:22])=[C:12]([O:11][CH2:9][CH3:10])[CH:13]=2)[CH2:2][CH2:3]1)[CH3:10]

Participants

3

Reactant 2

HCID 748473,4-DiethoxybenzaldehydeHCID 178511674HCID 178511674, compound

Product 1

HCID 178466602HCID 178466602, compoundYield 47%

Procedure

The title compound was prepared by a similar way as in Preparation Example 1, except that trans-1,4-cyclohexane diamine was used instead of trans-1,2-cyclohexane diamine and 3,4-diethoxybenzaldehyde was used instead of veratraldehyde.

Sources & evidence

ORD record
ord-7f06dad9fc6c4d83be41bf5d86e18b83
Source dataset
uspto-grants-1998_05
Patent number
US05756475

Reaction notes

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