HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate → HCID 15462892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-hydroxy-3-(2-methylprop-2-en-1-yl)benzoate | HCID 18705333 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15462892 | HCID 15462892 | — |
Reaction Steps
Ethyl 4-hydroxy-3-methallylbenzoate (25.5 g) was dissolved in ethanol (250 ml) and then, with 10% palladium charcoal (2.6 g) added thereto, this mixture was stirred at room temperature for 41 hours under a hydrogen gas atmosphere. After the reaction mixture was filtered, the filtrate was concentrated under a vacuum, thereby yielding 25.6 g of the aimed oily compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756505 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-defe1cfa150e48deb69b7ab091e9b3b9 |
| Source note | uspto-grants-1998_05 |