HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18354600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| Reactant | 3-Hydroxybenzamide | HCID 342403 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 18354600 | HCID 18354600 | — |
Reaction Steps
3-hydroxybenzamide (0.137 g; 1 mmol) was dissolved in anhydrous acetonitrile (20 ml) under a nitrogen atmosphere. To this was added potassium carbonate (0.138 g; 1 mmol) and 4-cyanobenzyl bromide (0.138 g; 1 mmol). This was left to reflux for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756510 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-50c39a28b2574d39be5b68f22df9cb8c |
| Source note | uspto-grants-1998_05 |