Thiazolidinedione → HCID 53945178, compound

HRID 1292186Notes

Reaction equation

[CH3:1][N:2]([CH2:12][CH2:13][CH2:14][CH2:15][O:16][C:17]1[CH:24]=[CH:23][C:20]([CH:21]=O)=[CH:19][CH:18]=1)[C:3]1[O:4][C:5]2[CH:11]=[CH:10][CH:9]=[CH:8][C:6]=2[N:7]=1.[S:25]1[CH2:29][C:28](=[O:30])[NH:27][C:26]1=[O:31]>>[CH3:1][N:2]([CH2:12][CH2:13][CH2:14][CH2:15][O:16][C:17]1[CH:24]=[CH:23][C:20]([CH:21]=[C:29]2[S:25][C:26](=[O:31])[NH:27][C:28]2=[O:30])=[CH:19][CH:18]=1)[C:3]1[O:4][C:5]2[CH:11]=[CH:10][CH:9]=[CH:8][C:6]=2[N:7]=1

Participants

Reactant 2

HCID 5437Thiazolidinedione

HCID 10041929HCID 10041929, compound

Product 1

HCID 53945178HCID 53945178, compound

Procedure

The title compound (m.p. 168° C.) was prepared from 4-[4-(N-methyl-N-(2-benzoxazolyl)amino)butoxy]benzaldehyde (3.5 g) and 2,4-thiazolidinedione (1.4 g) by a similar procedure to that described in Example 4.

Sources & evidence

ORD record: ord-8c03ca5c20df4b1ab1f479a9402109f2
Source dataset: uspto-grants-1998_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05756525

Reaction notes

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