Thioglycolic Acid → HCID 54532657, compound

HRID 1292367Notes

Reaction equation

HRID 1292367 reaction equation
Cl[CH2:2][O:3][CH2:4][CH2:5][O:6][CH3:7].[SH:8][CH2:9][C:10]([OH:12])=[O:11]>>[CH3:7][O:6][CH2:5][CH2:4][O:3][CH2:2][S:8][CH2:9][C:10]([OH:12])=[O:11]

Participants

3

Reactant 2

HCID 1133Thioglycolic AcidHCID 775901-(Chloromethoxy)-2-methoxyethane

Product 1

HCID 54532657HCID 54532657, compoundYield 58%

Procedure

In a similar manner, 2-methoxyethyl chloromethyl ether (4d) was reacted with mercaptoacetic acid to give S-(methoxy-ethoxy)methylmercaptoacetic acid (5d) in 58% yield as an oil.

Sources & evidence

ORD record
ord-e30d418b2202409eac3c453aac22e8c5
Source dataset
uspto-grants-1998_05
Patent number
US05756685

Reaction notes

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