HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-Hydroxy-N-benzimidazolon-5-yl-2-naphthamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | 3-Hydroxynaphthalene-2-carbonyl chloride | HCID 12896386 | — |
| Reactant | 5-amino-2H-1,3-benzodiazol-2-one | HCID 15250547 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3-Hydroxy-N-benzimidazolon-5-yl-2-naphthamide | HCID 20495683 | 86% |
Reaction Steps
CS 178560 describes the reaction of a solution of 3-hydroxy-2-naphthoyl chloride in toluene with 5-aminobenzimidazolone in the 30-fold amount of water in the presence of sodium acetate to give 3-hydroxy-N-benzimida-zolon-5-yl-2-naphthamide in 86% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756757 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-9b90926111044c6dbc82b2ffc0f95bdc |
| Source note | uspto-grants-1998_05 |