HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 15337896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 6-Octen-3-one, 2,4,4,7-tetramethyl- | HCID 9815427 | — |
| Product | HCID 15337896 | HCID 15337896 | — |
Reaction Steps
91 g of 2,4,4,7-tetramethyl-oct-6-en-3-one are stirred with 19 g of sodium borohydride in alcohol at 40° C. for 24 hours. The alcohol is distilled off, water is added and the product is extracted with tert-butyl methyl ether. The organic phase is washed neutral and distilled over a 40 cm packed column.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756821 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-fb84245fcbe54cecbe67af72aea2ad77 |
| Source note | uspto-grants-1998_05 |