Formic Acid → HCID 15337898, compound

HRID 1292591Notes

Reaction equation

HRID 1292591 reaction equation
[CH3:1][CH:2]([CH:4]([OH:13])[C:5]([CH3:12])([CH3:11])[CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])[CH3:3].[CH:14](O)=[O:15]>>[CH:14]([O:13][CH:4]([C:5]([CH3:11])([CH3:12])[CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])[CH:2]([CH3:1])[CH3:3])=[O:15]

Participants

3

Reactant 2

HCID 284Formic AcidHCID 15337896HCID 15337896, compound

Product 1

HCID 15337898HCID 15337898, compound

Procedure

52 g of 2,4,4,7-tetramethyl-oct-6-en-3-ol and 65 g of formic acid are stirred at 40° C. for 8 hours. The formic acid is then distilled off and the product is purified by cracking tube distillation.

Workup

  1. distillationThe formic acid is then distilled off
  2. customthe product is purified
  3. distillationdistillation

Sources & evidence

ORD record
ord-7034735c47894539b212c3d9c01683c8
Source dataset
uspto-grants-1998_05
Patent number
US05756821

Reaction notes

Loading…