Mesitylene → HCID 53855867, compound

HRID 1292626Notes

Reaction equation

HRID 1292626 reaction equation
[C:1]1([CH3:9])[CH:6]=[C:5]([CH3:7])[CH:4]=[C:3]([CH3:8])[CH:2]=1.[Cl-].[Al+3].[Cl-].[Cl-].[Cl:14][CH:15]=[CH:16][CH2:17]Cl>>[Cl:14][CH:15]=[CH:16][CH2:17][C:2]1[C:3]([CH3:8])=[CH:4][C:5]([CH3:7])=[CH:6][C:1]=1[CH3:9]

Participants

4

Reactant 3

HCID 7947MesityleneHCID 248831,3-DichloropropeneHCID 6451240Aluminum(III) Chloride

Product 1

HCID 53855867HCID 53855867, compound

Procedure

30 g (0.25 mol) of mesitylene and 0.7 g of aluminum chloride are introduced. 5.55 g (0.05 mol) of 1,3-dichloropropene (cis/trans) are then added dropwise at 20°-25° C. with cooling.

Workup

  1. temperaturewith cooling

Sources & evidence

ORD record
ord-2f1fad8f03e64bb7abf518181fc43041
Source dataset
uspto-grants-1998_05
Patent number
US05756858

Reaction notes

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