HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11074770, compound → HCID 58904459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11074770 | HCID 11074770 | — |
| Reactant | HCID 58904496 | HCID 58904496 | — |
| Product | HCID 58904459 | HCID 58904459 | 60.2% |
Reaction Steps
(±)-(S*)-(3,5-dimethoxy-phenoxy)-{(1S*)-2-[2-(3,5-dimethoxy-phenyl)-acetyl]-1-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl}-acetic acid (77 mg) is prepared in analogy to Example 5 starting from (±)-(S*)-(3,5-dimethoxy-phenoxy)-((1S*)-1-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-acetic acid (90 mg, 0.214 mmol, Example 1) and 3,5-dimethoxyphenylacetyl chloride (83 mg, 0.385 mmol). LC-MS2: tR=5.23 min, [M+1]+=598.35, [M−1]−=596.29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238685B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-ba1d5fbdf1c24b699ac9396c60b0e0cf |
| Source note | uspto-grants-2007_07 |