Methanesulfonyl chloride → 3-n-Propyloxetan-3-ylmethyl methanesulphonate

HRID 129283Notes

Reaction equation

[OH:1][CH2:2][C:3]1([CH2:7][CH2:8][CH3:9])[CH2:6][O:5][CH2:4]1.[CH3:10][S:11](Cl)(=[O:13])=[O:12]>>[CH3:10][S:11]([O:1][CH2:2][C:3]1([CH2:7][CH2:8][CH3:9])[CH2:6][O:5][CH2:4]1)(=[O:13])=[O:12]

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 1838902-Propyl-2-oxetanemethanol

Product 1

HCID 193734233-n-Propyloxetan-3-ylmethyl methanesulphonate

Procedure

3-n-Propyloxetan-3-ylmethyl methanesulphonate was prepared from 3-hydroxymethyl-3-n-propyloxetane and methanesulphonyl chloride using methodology outlined in stage i) of Example II.

Sources & evidence

ORD record: ord-1a1dc015e0a24d4aa27053f61d2cfef2
Source dataset: uspto-grants-1995_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05466710

Reaction notes

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