HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 23541921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | (2,4-Dichlorophenyl)boronic acid | HCID 2734659 | — |
| Reactant | HCID 23541998 | HCID 23541998 | — |
| Product | HCID 23541921 | HCID 23541921 | 50.2% |
Reaction Steps
The title compound (55.9 mg, 50%) was prepared by the method of Example 89 Step C from tert-butyl (±)-cis-2-bromo-4,5,7,8,10,10a-hexahydropyrido[4,3-b]pyrrolo[3,2,1-hi]indole-9(6aH)-carboxylate (94 mg, 0.25 mmol) and 2,4-dichlorophenylboronic acid (95 mg, 0.5 mmol) as a white amorphous solid. MS (CI, NH3): 445 (base, M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238690B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-acd371e4d76d454aa61a13803db9350c |
| Source note | uspto-grants-2007_07 |