HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 69433341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-Butene, 1-bromo-3-methyl- | HCID 70092 | — |
| Reactant | HCID 20576931 | HCID 20576931 | — |
| Product | HCID 69433341 | HCID 69433341 | — |
Reaction Steps
The title compound was prepared by the method of Example 382 as a yellow oil (27 mg, 76%) from (7aS,11aR)-2-(2,3-dichlorophenyl)-5,6,7a,8,9,10,11,11a-octahydro-4H-pyrido[3′,4′:4,5]pyrrolo[3,2,1-ij]quinoline (30 mg, 0.083 mmol) and 4-bromo-2-methyl-2-butene (25 mg, 0.17 mmol). MS (CI, NH3): 427.1 (base, M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238690B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-e09c1ab94b8a4fb3a7c5e8fbc88be121 |
| Source note | uspto-grants-2007_07 |