2-Propyl-2-oxetanemethanol → 1-(But-3-ynyloxymethyl)-4-n-propyl-2,6,7-trioxabicyclo[2.2.2]octane

HRID 129293Notes

Reaction equation

HRID 129293 reaction equation
[CH2:1]([O:5][CH2:6][C:7]([OH:9])=[O:8])[CH2:2][C:3]#[CH:4].[OH:10][CH2:11][C:12]1([CH2:16][CH2:17][CH3:18])[CH2:15]O[CH2:13]1>>[CH2:1]([O:5][CH2:6][C:7]12[O:10][CH2:11][C:12]([CH2:16][CH2:17][CH3:18])([CH2:15][O:9]1)[CH2:13][O:8]2)[CH2:2][C:3]#[CH:4]

Participants

3

Reactant 2

HCID 1838902-Propyl-2-oxetanemethanolHCID 193733742-(But-3-yn-1-yloxy)acetic acid

Product 1

HCID 193733271-(But-3-ynyloxymethyl)-4-n-propyl-2,6,7-trioxabicyclo[2.2.2]octane

Procedure

1-(But-3-ynyloxymethyl)-4-n-propyl-2,6,7-trioxabicyclo[2.2.2]octane was prepared from 2-(but-3-ynyloxy)acetic acid and 3-hydroxymethyl-3-n-propyl-oxetane using methodology described in Example I

Sources & evidence

ORD record
ord-8239007d14ad4b41a98068bf6f8c301e
Source dataset
uspto-grants-1995_11
Patent number
US05466710

Reaction notes

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