反应详情

A mixture of tropane (900 mg), 1-chloroethyl chloroformate (1 ml), and toluene (20 ml) was heated and refluxed for 6 hours. After that, methanol (10 ml) was added to the reaction solution, and further refluxed for 4 hours. The solvent was distilled to yield the title compound (850 mg).

1. temperaturewas heated
2. temperaturerefluxed for 6 hours
3. temperaturefurther refluxed for 4 hours
4. distillationThe solvent was distilled