HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2,5-Dichloronicotinate → Methyl 5-chloro-2-(3-cyanobenzyl)nicotinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2,5-Dichloronicotinate | HCID 2764318 | — |
| Reactant | HCID 178509756 | HCID 178509756 | — |
| Product | Methyl 5-chloro-2-(3-cyanobenzyl)nicotinate | HCID 57572315 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 58 from methyl 2,5-dichloronicotinate and 3-cyanobenzylzinc bromide: 1H-NMR (CDCl3) δ 8.66 (1H, d, J=2.5 Hz), 8.23 (1H, d, J=2.5 Hz), 7.58–7.34 (4H, m), 4.57 (2H, s), 3.91 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238714B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-4cc779f27e45411f824ebe4e756bdac8 |
| Source note | uspto-grants-2007_07 |