3,4-Dimethylphenol → HCID 69417266, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 45 from methyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate (step 1 of Example 48) and 3,4-dimethylphenol: 1H-NMR (CDCl3) δ 8.54 (1H, d, J=2.6 Hz), 8.26 (1H, d, J=7.4 Hz), 8.14 (1H, d, J=2.6 Hz), 8.00 (2H, dd, J=6.6, 1.8 Hz), 7.42 (2H, d, J=8.4 Hz), 7.22 (1H, d, J=8.1 Hz), 6.97–6.87 (2H, m), 5.42–5.32 (1H, m), 3.90 (3H, s), 2.29 (6H, s), 1.58 (3H, d, J=7.1 Hz).

Provenance & Evidence