2,4-Dichlorophenol → HCID 69416022, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 45 from methyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate (step 1 of Example 48) and 2,4-dichlorophenol: 1H-NMR (CDCl3) δ 8.54 (1H, d, J=2.6 Hz), 8.09–7.99 (4H, m), 7.52 (1H, d, J=2.3 Hz), 7.44 (2H, d, J=8.2 Hz), 7.36 (1H, dd, J=8.7, 2.4 Hz), 7.26 (1H, d, J=8.7 Hz), 5.44–5.34 (1H, m), 3.89 (3H, s), 1.61 (3H, d, J=6.9 Hz).

Provenance & Evidence