HCID 20298956, compound → HCID 69417827, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 3 of Example 1 from methyl 4-[(1S)-1-aminoethyl]benzoate hydrochloride (step 3 of Example 5) and 5-chloro-2-(3-methylphenoxy)benzoic acid (step 2): 1H-NMR (CDCl3) δ 8.18 (1H, d, J=2.6 Hz), 8.00–7.86 (3H, m), 7.40–7.20 (4H, m), 7.07–6.98 (1H, m), 6.98–6.74 (3H, m), 5.38–5.20 (1H, m), 3.88 (3H, s), 2.33 (3H, s), 1.48 (3H, d, J=6.9 Hz); MS (ESI) m/z 424 (M+H)+, 422 (M−H)−.

Provenance & Evidence