3-Chloro-5-methylphenol → HCID 69417691, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 45 from methyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate (step 1 of Example 48) and 3-chloro-5-methylphenol (J. Org. Chem. 1996, 61, 6814): 1H-NMR (CDCl3) δ 8.54 (1H, d, J=2.8 Hz), 8.15 (1H, d, J=2.6 Hz), 8.01 (3H, m), 7.42 (2H, d, J=8.1 Hz), 7.12 (1H, m), 6.97 (1H, m), 6.85 (1H, m), 5.36 (1H, m), 3.91 (3H, s), 2.38 (3H, s), 1.59 (3H, d, J=7.5 Hz).

Provenance & Evidence