3-Fluoro-2-methylphenol → HCID 69416295, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 45 from methyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate (step 1 of Example 48) and 3-fluoro-2-methylphenol: 1H-NMR (CDCl3) δ 8.57 (1H, d, J=2.3 Hz), 8.14 (1H, d, J=7.5 Hz), 8.10 (1H, d, J=2.3 Hz), 8.00 (2H, d, J=8.3 Hz), 7.43 (2H, d, J=8.3 Hz), 7.25 (1H, m), 7.03 (1H, t, J=8.3 Hz), 6.91 (1H, d, J=8.1 Hz), 5.40 (1H, m), 3.90 (3H, s), 2.06 (3H, s), 1.60 (3H, d, J=7.5 Hz).

Provenance & Evidence