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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 129335Generated: October 29, 2026

HCID 54290836, compound → HCID 19371039, compound

https://huagongshe.com/reaction/129335

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54290836HCID 54290836—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 19371039HCID 1937103982%

Reaction Steps

An ethanol solution (20 ml) of 3.05 g (10 mmol) of 5-(1-tetradecenyl)pyrrole-3-carboxylic acid prepared in the same manner as in Synthetic Example 7 was subjected to catalytic reduction for 2 hours in the presence of 300 mg of 10% palladium black. After removing the solvent the preduct was crystallized from heptane to obtain 2.50 g (82% yield) of a product identical to the one prepared in Example 4.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUSRE035096
Source datasetuspto-grants-1995_11
ORD IDord-acc9383d469547c5b7f81d0a00137098
Source noteuspto-grants-1995_11