HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54290836, compound → HCID 19371039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54290836 | HCID 54290836 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19371039 | HCID 19371039 | 82% |
Reaction Steps
An ethanol solution (20 ml) of 3.05 g (10 mmol) of 5-(1-tetradecenyl)pyrrole-3-carboxylic acid prepared in the same manner as in Synthetic Example 7 was subjected to catalytic reduction for 2 hours in the presence of 300 mg of 10% palladium black. After removing the solvent the preduct was crystallized from heptane to obtain 2.50 g (82% yield) of a product identical to the one prepared in Example 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE035096 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-acc9383d469547c5b7f81d0a00137098 |
| Source note | uspto-grants-1995_11 |