2-Methylpropylenediamine → HCID 18460863, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 1,2-diamino-2-methylpropane(3.14 mL, 30 mmol), and 6-chloronicotinonitrile (2.77 g, 20 mmol) were heated to 120° C. for 2 days. The reaction mixture was filtered, and the inorganic salt was rinsed with EtOAc. The filtrate was concentrated under reduced pressure to provide the titled compound as a pale yellow solid. MS (DCI) m/z 191 (M+H)+.

Provenance & Evidence