HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Bromobenzenesulphonyl chloride → HCID 8469449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Product | HCID 8469449 | HCID 8469449 | 93% |
Reaction Steps
Prepared by general procedure III from 3-Bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and 4-(2-Aminoethyl)-morpholine (2.80 mL, 22 mmol) to give the title compound (6.34 g, 93%) as a white solid. MS (ISN) 347.1 [(M−H)−], 349.3 [(M+2−H)−].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238808B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-8849e048cbdb4111964bf743ae865223 |
| Source note | uspto-grants-2007_07 |