HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 2-Chloro-4-methyl-1,3-thiazole-5-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 2-Chloro-4-methyl-1,3-thiazole-5-sulfonyl chloride | HCID 12094250 | — |
| Product | 2-Chloro-4-methyl-1,3-thiazole-5-sulfonamide | HCID 12094251 | 88.2% |
Reaction Steps
Prepared by general procedure III from 2-Chloro-4-methyl-thiazole-5-sulfonyl chloride (1.0 g, 4 mmol,) and ammonium hydroxide (0.32 mL, 4 mmol) to give 2-Chloro-4-methyl-thiazole-5-sulfonic acid amide (0.75 g, 81%) as awhite solid. MS (ISP) 213.0 [(M+H)+], 215.1 [(M+2+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238808B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-e8ce0b2ad7ed4f22a98e309b43d3d495 |
| Source note | uspto-grants-2007_07 |