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HRID1293814

反应详情

EQUATION

反应方程式

HRID 1293814 的结构方程式

REACTANTS

反应物

2
结构：CC(CO)(CO)NS(=O)(=O)c1cncc(Br)c1
HCID67000972

5-Bromo-N-[2-hydroxy-1-(hydroxymethyl)-1-methylethyl]-3-pyridinesulfonamide

C9H13BrN2O4S

结构：C#Cc1cnn2c(C3CC3)cc(-c3ccc(Cl)cc3)nc12
HCID86607996

未命名化合物

PRODUCTS

生成物

1
结构：CC(CO)(CO)NS(=O)(=O)c1cncc(C#Cc2cnn3c(C4CC4)cc(-c4ccc(Cl)cc4)nc23)c1
HCID67001063

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 5-(4-chloro-phenyl)-7-cyclopropyl-3-ethynyl-pyrazolo[1,5-a]pyrimidine (example C.5) (73 mg, 0.25 mmol) and 5-bromo-pyridine-3-sulfonic acid (2-hydroxy-1-hydroxymethyl-1-methyl-ethyl)-amide (81 mg, 0.25 mmol) (example B.4) according to general procedure II. Obtained as a yellow solid (68 mg, 50%). MS (ISP) 538.0 [(M+H)+]; mp 204–206° C.