HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoprene → 2-Methylbuta-1,3-diene--2-methylprop-1-ene (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoprene | HCID 6557 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Methylbuta-1,3-diene--2-methylprop-1-ene (1/1) | HCID 62703 | — |
Reaction Steps
The methodology of Example 3 was repeated, except that 1.5 mL of isoprene was added to the reaction vessel prior to initiation. The mixture was allowed to stir at −78° C. for 10 minutes, before addition of methanol (10 mL) to terminate the reaction. The yield of copolymer was 5.5 g (Mn=104,000, Mw=203,000). The isoprene content in the rubber was 1.5 mol-percent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238819B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-3c3de0c419514d8daadb65184fdf715d |
| Source note | uspto-grants-2007_07 |