Dipotassium tetrachloroplatinate → HCID 131726519, compound

HRID 1294045Notes

Reaction equation

HRID 1294045 reaction equation
[Cl:1][Pt-2:2](Cl)([Cl:4])[Cl:3].[K+].[K+].[CH:8]1([C:14]#[N:15])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>O>[Cl:1][Pt-:2]([Cl:4])[Cl:3].[CH:8]1([C:14]#[N:15])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1

Participants

4

Reactant 2

HCID 61440Dipotassium tetrachloroplatinateHCID 69834Cyanocyclohexane

Product 1

HCID 131726519HCID 131726519, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To a solution of (N(CH3)4)2[PtCl4] or K2[PtCl4] in 5 mL of deionized water will be added the cyclohexanecarbonitrile (1 mmol). The reaction mixture will then be stirred for approximately 10 days. Solid will be filtered, and the filtrate evaporated to dryness. A small amount of acetone will be added to the residue, and solid filtered. The filtrate will then be evaporated to obtain the desired product.

Workup

  1. filtrationSolid will be filtered
  2. customthe filtrate evaporated to dryness
  3. additionA small amount of acetone will be added to the residue, and solid
  4. filtrationfiltered
  5. customThe filtrate will then be evaporated

Sources & evidence

ORD record
ord-dcadef1a6db74985952f9c1a52d538bf
Source dataset
uspto-grants-2007_07
Patent number
US07238823B2

Reaction notes

Loading…