HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide diethylacetal → N,N-Dimethyl-2-(3-nitropyridin-4-yl)ethenamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide diethylacetal | HCID 70913 | — |
| Reactant | 4-Methyl-3-nitropyridine | HCID 521828 | — |
| Product | N,N-Dimethyl-2-(3-nitropyridin-4-yl)ethenamine | HCID 11063279 | — |
Reaction Steps
Commercially available 4-methyl-3-nitropyridine is condensed with N,N-dimethylformamide diethyl acetal to provide E-4-[2-(N,N-dimethylamino)-1-ethenyl]-3-nitropyridine, which is then subjected to catalytic hydrogenation to give 6-azaindole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05468757 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-e0d7c6e2ad1f47c78b58f92fa658c027 |
| Source note | uspto-grants-1995_11 |