HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trihydroxybenzaldehyde → HCID 136380446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trihydroxybenzaldehyde | HCID 68099 | — |
| Reactant | N-(Naphthalen-1-yl)hydrazinecarbothioamide | HCID 2760175 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 136380446 | HCID 136380446 | 54% |
Reaction Steps
A solution of 4-(naphth-1-yl)thiosemicarbazide (572 mg, 2.63 mmol) and 2,4,6-trihydroxybenzaldehyde (405 mg, 2.63 mmol) in acetic acid (5 mL) was heated under reflux for 20 min, then cooled. The precipitate was filtered, washed (acetic acid) and dried to give the title compound (445 mg, 54%) as a solid. MS (ES+) m/e 354 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241783B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-5d878955377d46e0b30124adea33c3aa |
| Source note | uspto-grants-2007_07 |