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HRID1294798

反应详情

EQUATION

反应方程式

HRID 1294798 的结构方程式

REACTANTS

反应物

2
结构：Brc1cnc2ccccc2c1
HCID21413

Quinoline, 3-bromo-

C9H6BrN

结构：CC(C)(C)OC(=O)N1CCNCC1
HCID143452

tert-Butyl piperazine-1-carboxylate

C9H18N2O2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCN(c2cnc3ccccc3c2)CC1
HCID58906302

未命名化合物

PROCEDURE

实验过程

Prepared in analogy to example 1.16 (a) from 3-bromoquinoline and piperazine-1-carboxylic acid tert-butyl ester. Chromatography (SiO2; cyclohexane/ethyl acetate 1/1), followed by crystallization from diethyl ether/cyclohexane yields the title product as a colorless solid.

WORKUP

后处理

  1. customChromatography (SiO2; cyclohexane/ethyl acetate 1/1), followed by crystallization from diethyl ether/cyclohexane