HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 58970540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | (S)-2-(1-Methyl-2,2,2-trifluoroethoxy)-5-methylsulfonylbenzoic acid | HCID 58863351 | — |
| Reactant | 6-Chloro-2-piperazin-1-yl-quinoline hydrochloride | HCID 68896684 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 58970540 | HCID 58970540 | — |
Reaction Steps
Prepared in analogy to example 1.1 b) from 6-chloro-2-piperazin-1-yl-quinoline hydrochloride (Example 1.20b) and 5-methanesulfonyl-2-((S)-2,2,2-trifluoro-1-methyl-ethoxy)-benzoic acid (Example 2.7) in acetonitrile. Chromatography (SiO2; ethyl acetate) yields the title compound as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241761B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-f007763a74bc4e3fa84a115fb3f87eb3 |
| Source note | uspto-grants-2007_07 |